●Part 1 Experimental Organic Chemistry Chapter 1 General Introduction 3 1. Laboratory Rules. 3 2. Safety Rules and Regulations in Chemistry Laboratory . 3 3. Treatment of the Common Accidents in Laboratory. 5 4. Fire Prevention and Treatment . 5 5. First Aid Kit 5 6. Preview, Record and Laboratory Report. 5 Chapter 2 Common laboratory Apparatus and Equipment . 7 1. General Glassware 7 2. Common Standard-taper Glassware 7 3. Common Glass Apparatus. 8 4. Common Equipment 8 Chapter 3 Laboratory Experiments 11 Experiment 1 Basic Laboratory Techniques (Ⅰ) . 11 Experiment 2 Basic Laboratory Techniques (Ⅱ) . 14 Experiment 3 Extraction of Iodine. 16 Experiment 4 Determination of the Melting Point 18 Experiment 5 Micro Determination of the Boiling Point 19 Experiment 6 Refractive Index Determination of Liquid Organic Compound 21 Experiment 7 Operation of Organic Molecular Models. 23 Experiment 8 Paper Electrophoresis of Amino Acid 25 Experiment 9 Column Chromatography 27 Experiment 10 Thin-Layer Chromatography (TLC) . 29 Experiment 11 Paper Chromatography 31 Experiment 12 Preparation of Aspirin 34 Experiment 13 Preparation of Acetanilide . 36 Experiment 14 Extraction of Rutin and Recovery of Extraction Agent 38 Experiment 15 Analysis of Unknown Sample of Organic Compounds (Designing Experiment). 39 Part 2 Solutions Manual for Organic Chemistry Chapter Introduction 43 Chapter Saturated Hydrocarbons: Alkanes and Cycloalkanes . 45 Chapter Unsaturated Hydrocarbons: Alkenes, Alkynes and Aromatics. 48 Chapter Alcohols, Phenols, and Ethers 51 Chapter Aldehydes and Ketones . 55 Chapter Carboxylic Acids and Acid Derivatives. 59 Chapter Amines . 64 Chapter Optical Isomerism 66 Chapter Carbohydrate. 70 Chapter Lipids. 73 Chapter Proteins . 76 Chapter Nucleic Acids 79 References 80
